Synthesis and Structure of Barium Hexaferrite BaFe12–xInxO19 (x = 0–1)

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Аннотация

This study presents the results of the synthesis and examination of indium-substituted barium hexaferrite samples with the formula BaFe12–xInxO19. The ferrites were obtained via a solid state synthesis method. The substitution level of indium, represented by x(In), was varied from 0 to 1 in 0.25 increments. The stoichiometric formulas of the compounds were calculated using the EDS data. The powder X-ray diffraction analysis indicated that all samples form a single crystalline phase with the M-type hexaferrite structure. Parameters of the crystal unit cell were calculated from powder diffraction data. An expansion of the crystal lattice parameters was observed as iron was substituted with indium, from x = 0 to x = 0.84. The Curie temperatures of the synthesized ferrites were determined using differential scanning calorimetry (DSC) method. It is established that the Curie temperature decreases from 452 to 292°C with In content growth from x = 0 to x = 0.84 in the BaFe12–xInxO19.

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Авторлар туралы

A. Punda

South Ural State University (National Research University)

Хат алмасуға жауапты Автор.
Email: pundaai@susu.ru
Ресей, Chelyabinsk, 454080

K. Gafarov

South Ural State University (National Research University)

Email: pundaai@susu.ru
Ресей, Chelyabinsk, 454080

V. Zhivulin

South Ural State University (National Research University)

Email: pundaai@susu.ru
Ресей, Chelyabinsk, 454080

A. Chernukha

South Ural State University (National Research University); Moscow Institute of Physics and Technology (National Research University)

Email: pundaai@susu.ru
Ресей, Chelyabinsk, 454080; Dolgoprudny, 141701

A. Zykova

South Ural State University (National Research University)

Email: pundaai@susu.ru
Ресей, Chelyabinsk, 454080

S. Gudkova

South Ural State University (National Research University); Moscow Institute of Physics and Technology (National Research University)

Email: pundaai@susu.ru
Ресей, Chelyabinsk, 454080; Dolgoprudny, 141701

L. Pesin

South Ural State University (National Research University)

Email: pundaai@susu.ru
Ресей, Chelyabinsk, 454080

G. Vyatkin

South Ural State University (National Research University)

Email: pundaai@susu.ru
Ресей, Chelyabinsk, 454080

D. Vinnik

South Ural State University (National Research University); Moscow Institute of Physics and Technology (National Research University); St. Petersburg State University

Email: pundaai@susu.ru
Ресей, Chelyabinsk, 454080; Dolgoprudny, 141701; St. Petersburg, 199034

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2. Fig. 1. Dependence of the indium content in the synthesized material on its content in the initial charge.

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3. Fig. 2. Diffractograms of BaFe12–xInxO19 solid solutions. The red bar chart indicates the literature data for BaFe12O19 [48].

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4. Fig. 3. Parameters of the elementary crystal cell of BaFe12–xInxO19. 1 – a (Å), 2 – c (Å), 3 – V (Å3) solid solutions.

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5. Fig. 4. Curie point values for solid solutions BaFe12–xInxO19 (error -2 °C).

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